Titration Experiment Write-up

 

Lab Notebook

Procedure – reference the handout; be sure to include any changes.

 

Data – a clear record of your data collection.  All volume measurements should have been recorded to two decimal places off of your buret.

 

Lab book format – signature, stamp, etcÉ

 

 

Informal Report

Title page with name, date, experiment title, and section #

Cut and paste the grading rubric at the base of this document on the title page

 

Objective-What is the major goal(s) of this experiment?  Be sure to be specific, but limit your objective to 3-4 sentences maximum.

 

Results and calculation section – Report your average gram molar mass with standard deviation and average melting point.  Show your calculations.  These may be typed or handwritten.  Note any unusual or unexpected observations in the experiment.

 

Discussion– State the identity of your unknown acid.  Discuss how you came to that conclusion using your average gram molar mass with standard deviation and average melting point range to justify your identification.  Explain how you narrowed down the suspects and state your second choice and/or third choice, if appropriate and how they were eliminated.  Be sure to discuss, how many standard deviations the actual molar mass of the acid you believe best represents your unknown is away from the experimental molecular mass of the acid.  Also, does the actual melting point of your identified acid fall within the range of your experimental average melting points?  Explain why or why not.  Discuss the accuracy and precision of your average gram molar mass and melting point.  Discuss any sources of error that may have occurred in the experiment.  For example, if you added too much base to one of your titrations, you should identify how that would have affected your gram molar mass calculation.   

 

Conclusion-Evaluate the objective of the experiment and restate the identity of your unknown acid, the average gram molar mass and the average melting point range.

 

Questions - Complete the post lab questions at the end of the experiment. 

 

 

 

Titration Experiment – Grading Rubric

 

 

Lab Book

 

/15

Procedure/Format

/8

 

Data

/7

 

Informal Report

 

/60

Title Page

/2

 

Objective

/5

 

Results and Calculations

/13

 

Discussion

/15

 

Conclusion

/10

 

Questions

/15

 

Computer Printout

 

/25

Total

 

/100